Paper 7.2

Phase Equilibria in the Co-Cu-Si-O System

 

Zabdyr Leszek A.1 and Fabrichnaya Olga B.2

 

1Institute of Metallurgy and Materials Science, Polish Academy of Sciences, Krakow, Poland

2Max Planck Institute, Stuttgart, Germany.

 

The thermodynamic description of liquid and fcc phase in the Co-O system is obtained using available  experimental data on oxygen dissolution in solid and liquid cobalt (see references in [03Che]. Thermodynamic properties of liquid are determined in the system cobalt oxide-copper oxide  using experimental data of [68Dri] and [69Lan]. The experimental data [68Dri] and [69Lan] contradict each other. Depending on value of mixing parameters of liquid phase two data sets consistent with phase relations of [68Dri] or [69Lan] are obtained.

 

Combining data on ternary systems the thermodynamic description of solid phases in the Co-Cu-Si-O system is obtained. The mixing parameters of olivine and the Gibbs energy of fictive Cu2SiO4 end-member are subjected to optimisation procedure using experimental data on Co/Cu partitioning between olivine and (Co,Cu)O phase with halite structure obtained in this study. It is shown that several sets equally well describing experimental results are possible. The knowledge about Co/Cu partitioning between olivine and (Cu, Co)O phase with structure of CuO in equilibrium with SiO2 is crucial to constrain thermodynamic parameters for olivine.

 

References

[68Dri]       F.C.M. Driessens, G.D. Rieck, H.N. Coenen: J. Inorg. Nucl. Chem. 30 (1968) 743-753.

[69Lan]      C. Landolt, A. Muan: J. Inorg. Nucl. Chem. 31 (1969) 1319-1326.

[03Che]     M. Chen, B. Hallstedt, L.J. Gauckler: J. Phase Equilibria 24 (2003) 212-226.